Electroanalytical Methods in Pharmaceutical Analysis and Their Validation

Sibel A. Ozkan

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October 2011
350 pp.
(hardcover)

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Illustrated:
ISBN: 978-0-9664286-7-4

 

 

Contents

Preface

1. Drugs Versus Chemicals: Similarities and Differences

Arzu Onay-Besikci and Sibel A. Ozkan

1.1. Peripheral Nervous System Drugs

1.2. Central Nervous System Drugs

1.3. Cardiovascular and Renal Drugs

1.4. Endocrine Drugs

1.5. Chemotherapeutic Drugs

1.6. Anti-inflammatory, Antiallergic, and Immunoregulatory Drugs

1.7. Development of Drugs

References

2. Electroanalytical Chemistry

Sibel A. Ozkan

References

3. Experimental Considerations

Sibel A. Ozkan

3.1. Reference Electrode

3.2. Auxiliary (Counter) Electrode

3.3. Electroanalytical Conditions

References

4. Working Electrodes

Sibel A. Ozkan

4.1. Mercury Electrodes

4.1.1. Dropping Mercury Electrodes

4.1.2. Hanging Mercury Drop Electrodes

4.1.3. Static Mercury Drop Electrodes

4.1.4. Mercury Film Electrodes

4.2. Solid Electrodes

4.2.1. Noble Metal Electrodes

4.2.2. Carbon Electrodes

4.2.2.1. Graphite Electrodes

4.2.2.2. Fullerene and Carbon Nanotube Electrodes

4.2.2.3. Carbon Fibers

4.2.2.4. Screen-Printed Electrodes

4.2.2.5. Carbon Paste Electrodes

4.2.2.6. Glassy Carbon Electrodes

4.2.2.7. Diamond Electrodes

4.2.2.8. Chemically Modified Electrodes

References

5. Classical Potential Sweep Methods in Pharmaceutical
Analysis

Sibel A. Ozkan

5.1. Applications of LSV in Pharmaceutical Analysis

5.2. Applications of CV in Pharmaceutical Analysis

5.3. Summary

References

6. Controlled Potential and Pulsed Voltammetric
Techniques in Pharmaceutical Analysis

Bengi Uslu and Sibel A. Ozkan

6.1. Polarography

6.2. Pulse Polarography/Voltammetry

6.2.1. Normal Pulse Voltammetry/Polarography

6.2.2. AC Voltammetry/ Polarography

6.2.3. Differential Pulse Polarography/Voltammetry (DPV)

6.2.4. Square-Wave Voltammetry

6.2.5. Staircase Voltammetry

References

7. Stripping Techniques in Pharmaceutical Analysis

Sibel A. Ozkan

7.1. Anodic Stripping Voltammetry

7.2. Cathodic Stripping Voltammetry

7.3. Adsorptive Stripping Voltammetry

7.4. Potentiometric Stripping Analysis

7.5. Abrasive Stripping Voltammetry

References

8. Practical Applications in Pharmaceutical and
Biomedical Chemistry

Sibel Suzen and Sibel A. Ozkan

8.1. Electrochemistry in Drug Development and Analysis

8.1.1. Benzimidazoles

8.1.2. Indoles

8.1.3. Catechols

8.1.4. Benzofuran

8.1.5. Quinones

8.1.6. Antibiotics

8.1.7. Steroids

8.1.8. Other Drug Molecules

8.2. Metabolite Determination Using Electrochemical Methods

8.3. Oxidative Stress

8.4. Electrochemical Therapy

References

9. Method Validation

Sibel A. Ozkan

9.1. Validation Processes of Electroanalytical Methods

9.2. Validation Characteristics of Electroanalytical Methods

9.2.1. Specificity and Selectivity

9.2.2. Linearity

9.2.3. Range

9.2.4. Sensitivity

9.2.5. Limit of Detection

9.2.6. Limit of Quantitation

9.2.7. Accuracy

9.2.8. Precision

9.2.9. Robustness

9.2.10. Ruggedness

9.2.11. Stability

References

Abbreviations and Symbols

Index

Preface | About the Author

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